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A One-pot Synthesis of Terminal Alkynes from anti-3-Aryl-2,3-dibromopropanoic Acids under Microwave Irradiation

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Title: A One-pot Synthesis of Terminal Alkynes from anti-3-Aryl-2,3-dibromopropanoic Acids under Microwave Irradiation
Authors: Kuang, Chunxiang Browse this author
Senboku, Hisanori Browse this author →KAKEN DB
Tokuda, Masao Browse this author
Keywords: terminal alkynes
microwave irradiation
Issue Date: 5-Jan-2005
Publisher: Chemical Society of Japan
Journal Title: Chemistry Letters
Volume: 34
Issue: 1
Start Page: 28
End Page: 29
Publisher DOI: 10.1246/cl.2005.28
Abstract: A facile one-pot synthesis of terminal alkynes was achieved by microwave irradiation of a mixture of anti-3-aryl-2,3-dibromopropanoic acids, Et3N and DMF and subsequent irradiation in the presence of 1,8-diazabicyclo[5.4.0]undec-7-ene (DBU). This method requires short reaction time (1–2 min) and gives terminal alkynes in high yields.
Type: article
URI: http://hdl.handle.net/2115/70910
Appears in Collections:工学院・工学研究院 (Graduate School of Engineering / Faculty of Engineering) > 雑誌発表論文等 (Peer-reviewed Journal Articles, etc)

Submitter: 仙北 久典

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