Micro-liquid enclosure array and its semi-automated assembling system for x-ray free-electron laser diffractive imaging of samples in solution

Kimura, Takashi; Suzuki, Akihiro; Yang, Ying; Niida, Yoshiya; Nishioka, Akiko; Takei, Masashi; Wei, Jinjian; Mitomo, Hideyuki; Matsuo, Yasutaka; Niikura, Kenichi; Ijiro, Kuniharu; Tono, Kensuke; Yabashi, Makina; Ishikawa, Tetsuya; Oshima, Tairo; Bessho, Yoshitaka; Joti, Yasumasa; Nishino, Yoshinori

Micro-liquid enclosure array and its semi-automated assembling system for x-ray free-electron laser diffractive imaging of samples in solution

Kimura, Takashi; Suzuki, Akihiro; Yang, Ying et al.

Review of Scientific Instruments, 2020, 91(8), 083706

Permalink : https://hdl.handle.net/2115/81826

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アクセス権	open access
URI	https://hdl.handle.net/2115/81826
タイトル	Micro-liquid enclosure array and its semi-automated assembling system for x-ray free-electron laser diffractive imaging of samples in solution
著者	Kimura, Takashi ; Suzuki, Akihiro ; Yang, Ying ; Niida, Yoshiya ; Nishioka, Akiko ; Takei, Masashi ; Wei, Jinjian ; Mitomo, Hideyuki ; Matsuo, Yasutaka ; Niikura, Kenichi ; Ijiro, Kuniharu ; Tono, Kensuke ; Yabashi, Makina ; Ishikawa, Tetsuya ; Oshima, Tairo ; Bessho, Yoshitaka ; Joti, Yasumasa ; Nishino, Yoshinori
著者名 Kimura, Takashi
e-Rad_Researcher 20781850 著者名 Suzuki, Akihiro
著者名 Yang, Ying
著者名 Niida, Yoshiya
著者名 Nishioka, Akiko
著者名 Takei, Masashi
著者名 Wei, Jinjian
e-Rad_Researcher 50564952 著者名 Mitomo, Hideyuki
e-Rad_Researcher 90374652 著者名 Matsuo, Yasutaka
e-Rad_Researcher 40360896 著者名 Niikura, Kenichi
e-Rad_Researcher 90221762 著者名 Ijiro, Kuniharu
e-Rad_Researcher 00353508 著者名 Tono, Kensuke
e-Rad_Researcher 00372144 著者名 Yabashi, Makina
e-Rad_Researcher 80159699 著者名 Ishikawa, Tetsuya
著者名 Oshima, Tairo
e-Rad_Researcher 70242815 著者名 Bessho, Yoshitaka
e-Rad_Researcher 30360415 著者名 Joti, Yasumasa
e-Rad_Researcher 40392063 著者名 Nishino, Yoshinori
言語	英語
発行日	2020-08-01
出版者	American Institute of Physics (AIP)
収録物名	Review of Scientific Instruments
巻(号)	91(8)
ページ	083706
抄録	We developed micro-liquid enclosure arrays (MLEAs) for holding solution samples in coherent diffractive imaging (CDI) using x-ray free-electron lasers (XFELs). Hundreds of fully isolated micro-liquid enclosures are arranged in a single MLEA chip for efficient measurement, where each enclosure is destroyed after exposure to a single XFEL pulse. A semi-automated MLEA assembling system was also developed to enclose solution samples into MLEAs efficiently at high precision. We performed XFEL-based CDI experiments using MLEAs and imaged in-solution structures of self-assembled gold nanoparticles. The sample hit rate can be optimized by adjusting solution concentration, and we achieved a single-particle hit rate of 31%, which is not far from the theoretical upper limit of 37% derived from the Poisson statistics. MELAs allow us to perform CDI measurement under controlled solution conditions and will help reveal the nanostructures and dynamics of particles in solution.
資源タイプ	学術雑誌論文
出版タイプ	Accepted Manuscript
権利情報	This article may be downloaded for personal use only. Any other use requires prior permission of the author and AIP Publishing. This article appeared in (Takashi Kimura, Akihiro Suzuki, Ying Yang, Yoshiya Niida, Akiko Nishioka, Masashi Takei, Jinjian Wei, Hideyuki Mitomo, Yasutaka Matsuo, Kenichi Niikura, Kuniharu Ijiro, Kensuke Tono, Makina Yabashi, Tetsuya Ishikawa, Tairo Oshima, Yoshitaka Bessho, Yasumasa Joti, and Yoshinori Nishino , "Micro-liquid enclosure array and its semi-automated assembling system for x-ray free-electron laser diffractive imaging of samples in solution", Review of Scientific Instruments 91, 083706 (2020) https://doi.org/10.1063/5.0008398) and may be found at (https://aip.scitation.org/doi/10.1063/5.0008398)
PISSN	0034-6748
関連情報 (isVersionOf)	出版社版DOI https://doi.org/10.1063/5.0008398