| Title: | A high-temperature in situ cell with a large solid angle for fluorescence X-ray absorption fine structure measurement |
| Authors: | Murata, Naoyoshi Browse this author |
| Kobayashi, Makoto Browse this author |
| Okada, Yukari Browse this author |
| Suzuki, Takuya Browse this author |
| Nitani, Hiroaki Browse this author |
| Niwa, Yasuhiro Browse this author |
| Abe, Hitoshi Browse this author |
| Wada, Takahiro Browse this author |
| Mukai, Shingo Browse this author |
| Uehara, Hiromitsu Browse this author |
| Ariga, Hiroko Browse this author |
| Takakusagi, Satoru Browse this author →KAKEN DB |
| Asakura, Kiyotaka Browse this author →KAKEN DB |
| Issue Date: | Mar-2015 |
| Publisher: | American Institute of Physics |
| Journal Title: | Review of scientific instruments |
| Volume: | 86 |
| Issue: | 3 |
| Start Page: | 034102-1 |
| End Page: | 034102-6 |
| Publisher DOI: | 10.1063/1.4914459 |
| PMID: | 25832248 |
| Abstract: | We present the design and performance of a high-temperature in situ cell with a large solid angle for fluorescence X-ray absorption fine structure (XAFS) spectra. The cell has a large fluorescence XAFS window (116 mm(phi)) near the sample in the cell, realizing a large half-cone angle of 56 degrees. We use a small heater (25 x 35 mm(2)) to heat the sample locally to 873 K. We measured a Pt-SnO2 thin layer on a Si substrate at reaction conditions having a high activity. In situ measurement enables the analysis of the difference XAFS spectra between before and during the reaction to reveal the structure change during the operation. (C) 2015 AIP Publishing LLC. |
| Rights: | Copyright 2015 American Institute of Physics. This article may be downloaded for personal use only. Any other use requires prior permission of the author and the American Institute of Physics. The following article appeared in Review of Scientific Instruments and may be found at http://scitation.aip.org/content/aip/journal/rsi/86/3/10.1063/1.4914459 |
| Type: | article |
| URI: | http://hdl.handle.net/2115/59168 |
| Appears in Collections: | 触媒科学研究所 (Institute for Catalysis) > 雑誌発表論文等 (Peer-reviewed Journal Articles, etc)
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