Practical Synthesis of Dirhodium (II) Tetrakis[N-phthaloyl-(S)-tert-leucinate]


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Please use this identifier to cite or link to this item:http://hdl.handle.net/2115/26434

Title:	Practical Synthesis of Dirhodium (II) Tetrakis[N-phthaloyl-(S)-tert-leucinate]
Authors:	Tsutsui, Hideyuki Browse this author
	Abe, Takumi Browse this author
	Nakamura, Seiichi Browse this author
	Anada, Masahiro Browse this author →KAKEN DB
	Hashimoto, Shunichi Browse this author →KAKEN DB
Keywords:	tert-leucine
	N-phthaloylation
	dirhodium(II)
	carboxylate
	chiral catalyst
Issue Date:	1-Oct-2005
Publisher:	社団法人　日本薬学会
Journal Title:	Chemical & pharmaceutical bulletin
Volume:	53
Issue:	10
Start Page:	1366
End Page:	1368
Abstract:	An efficient and reliable procedure for the preparation of dirhodium(II) tetrakis[N-phthaloyl-(S)-tert-leuci-nate], Rh_2(S-PTTL)_4, a universally effective catalyst for a range of enantioselective carbene transformations, is described. The N-phthaloylation of (S)-tert-leucine by the method of Bose with essentially no racemization is a key to this process.
Type:	article
URI:	http://hdl.handle.net/2115/26434
Appears in Collections:	薬学研究院 (Faculty of Pharmaceutical Sciences) > 雑誌発表論文等 (Peer-reviewed Journal Articles, etc)

Submitter: 穴田仁洋

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