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Direct and stereoselective synthesis of 2-azido-2-deoxy-β-D-mannosides using the phosphate method

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Title: Direct and stereoselective synthesis of 2-azido-2-deoxy-β-D-mannosides using the phosphate method
Authors: Nakamura, Seiichi1 Browse this author
Tsuda, Toshifumi2 Browse this author
Suzuki, Noritoshi3 Browse this author
Hashimoto, Shunichi4 Browse this author →KAKEN DB
Authors(alt): 中村, 精一1
津田, 敏史2
鈴木, 規敏3
橋本, 俊一4
Issue Date: 1-Feb-2009
Publisher: The Japan Institute of Heterocyclic Chemistry
Journal Title: Heterocycles
Volume: 77
Issue: 2
Start Page: 843
End Page: 848
Publisher DOI: 10.3987/COM-08-S(F)108
Abstract: TMSOTf-promoted glycosidation of 2-azido-3-O-benzyl-4,6-O-benzylidene-2-deoxy-α-D-mannosyl diphenyl phosphate with a variety of acceptor alcohols in CH2Cl2 at -30℃ in the presence of pulverized 4-Å molecular sieves (MS) afforded 2-azido-2-deoxy-β-mannosides in high yields and with good to high β-selectivities.
Type: article (author version)
URI: http://hdl.handle.net/2115/35613
Appears in Collections:薬学研究院 (Faculty of Pharmaceutical Sciences) > 雑誌発表論文等 (Peer-reviewed Journal Articles, etc)

Submitter: 中村 精一

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