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Preparation of Ag nanoparticles using hydrogen peroxide as a reducing agent
Title: | Preparation of Ag nanoparticles using hydrogen peroxide as a reducing agent |
Authors: | Nishimoto, Masamu Browse this author | Abe, Shigeaki Browse this author | Yonezawa, Tetsu Browse this author →KAKEN DB |
Issue Date: | 7-Sep-2018 |
Publisher: | Royal Society of Chemistry |
Journal Title: | New journal of chemistry |
Volume: | 42 |
Issue: | 17 |
Start Page: | 14493 |
End Page: | 14501 |
Publisher DOI: | 10.1039/c8nj01747f |
Abstract: | Herein, we report a method for Ag nanoparticle preparation using hydrogen peroxide as a reducing agent. Ag nanoparticles were synthesized using silver(i) nitrate as a silver precursor, aqueous NH3 as a pH adjustor, and poly(vinyl pyrrolidone) (PVP) as a dispersant. The PVP concentration, the reaction temperature, the pH of the reaction solution, and the silver precursor all have a great influence on the size of the Ag nanoparticles. These parameters affected the reduction speed of the Ag+ ions and the aggregation of Ag nanoparticles. Ag nanoparticles of uniform shape were obtained under optimized conditions. In this work, we discuss a Ag nanoparticle growth mechanism based on La Mer's model, and aggregation control using PVP. This is a promising Ag nanoparticle preparation method with a low environmental load. Antibacterial tests using the obtained Ag nanoparticles were also carried out. |
Type: | article (author version) |
URI: | http://hdl.handle.net/2115/75420 |
Appears in Collections: | 工学院・工学研究院 (Graduate School of Engineering / Faculty of Engineering) > 雑誌発表論文等 (Peer-reviewed Journal Articles, etc)
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Submitter: 米澤 徹
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