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Application of non-destructive integrated CT-XRD method to investigate alteration of cementitious materials subjected to high temperature and pure water

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Title: Application of non-destructive integrated CT-XRD method to investigate alteration of cementitious materials subjected to high temperature and pure water
Authors: Takahashi, Hayato Browse this author
Sugiyama, Takafumi Browse this author →KAKEN DB
Keywords: Non-destructive integrated CT-XRD method
Microstructure
Cement hydration system
High temperature
Rehydration
Leaching
Issue Date: 10-Apr-2019
Publisher: Elsevier
Journal Title: Construction and building materials
Volume: 203
Start Page: 579
End Page: 588
Publisher DOI: 10.1016/j.conbuildmat.2019.01.128
Abstract: In order to analyze the alteration mechanism after the exposure to various maximum temperatures and immersion in pure water, non-destructive integrated CT-XRD method (the CT-XRD) was applied. Firstly, the verification of the CT-XRD was carried out to compare with conventional powder X-ray diffraction. It revealed that the CT-XRD could evaluate the crystals properly with a given limitation for low energy band. Besides, the CT-XRD indicated the advantage that can detect the presence of crystals which cannot be detected after grinding in preparing the powder sample for the conventional powder XRD. Then, the carbonated cement paste that was heated at 200, 400, 600, and 800 degrees C followed by immersion in pure water was evaluated by the CT-XRD. The results suggest that sample heated at 400 degrees C showed the resistance of leaching at most. In addition, rehydration of clinker minerals generated due to heating at 800 degrees C could be identified although the hydration product was easily dissolved into water.
Rights: © 2019. This manuscript version is made available under the CC-BY-NC-ND 4.0 license http://creativecommons.org/licenses/by-nc-nd/4.0/
http://creativecommons.org/licenses/by-nc-nd/4.0/
Type: article (author version)
URI: http://hdl.handle.net/2115/80961
Appears in Collections:工学院・工学研究院 (Graduate School of Engineering / Faculty of Engineering) > 雑誌発表論文等 (Peer-reviewed Journal Articles, etc)

Submitter: 高橋 駿人

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