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Electrochemical In Situ/operando Spectroscopy and Microscopy Part 1 : Fundamentals
Title: | Electrochemical In Situ/operando Spectroscopy and Microscopy Part 1 : Fundamentals |
Authors: | Matsui, Masaki Browse this author →KAKEN DB | Orikasa, Yuki Browse this author | Uchiyama, Tomoki Browse this author | Nishi, Naoya Browse this author | Miyahara, Yuto Browse this author | Otoyama, Misae Browse this author | Tsuda, Tetsuya Browse this author |
Keywords: | Spectroelectrochemistry | In Situ/operando Spectroscopy and Microscopy | In Situ Cell Design | Measurement Tips |
Issue Date: | 31-Oct-2022 |
Publisher: | The Electrochemical Society of Japan |
Journal Title: | Electrochemistry |
Volume: | 90 |
Issue: | 10 |
Start Page: | 102009 |
Publisher DOI: | 10.5796/electrochemistry.22-66093 |
Abstract: | Spectroscopic and microscopic techniques are complementary to electrochemical studies because electrochemical data consists of current, voltage and time, and has no direct information concerning the chemical structure of active species. Hence electrochemical in situ/operando spectroscopy and microscopy become powerful tools for identification of the electrochemically active species during the electrochemical reactions. The present comprehensive paper provides the fundamental theory, cell design concepts, and measurement tips of various spectroscopic and microscopic techniques. X-ray absorption spectroscopy, infrared spectroscopy, surface plasmon resonance, Raman spectroscopy, confocal microscopy and electron microscopy are covered in the present paper. The introduced cell design becomes the critical part for chemists and materials scientists to start these measurements. Several advanced techniques from recent studies are also introduced. (C) The Author(s) 2022. Published by ECSJ. |
Type: | article |
URI: | http://hdl.handle.net/2115/87527 |
Appears in Collections: | 理学院・理学研究院 (Graduate School of Science / Faculty of Science) > 雑誌発表論文等 (Peer-reviewed Journal Articles, etc)
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