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Electrochemical In Situ/operando Spectroscopy and Microscopy Part 1 : Fundamentals

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Title: Electrochemical In Situ/operando Spectroscopy and Microscopy Part 1 : Fundamentals
Authors: Matsui, Masaki Browse this author →KAKEN DB
Orikasa, Yuki Browse this author
Uchiyama, Tomoki Browse this author
Nishi, Naoya Browse this author
Miyahara, Yuto Browse this author
Otoyama, Misae Browse this author
Tsuda, Tetsuya Browse this author
Keywords: Spectroelectrochemistry
In Situ/operando Spectroscopy and Microscopy
In Situ Cell Design
Measurement Tips
Issue Date: 31-Oct-2022
Publisher: The Electrochemical Society of Japan
Journal Title: Electrochemistry
Volume: 90
Issue: 10
Start Page: 102009
Publisher DOI: 10.5796/electrochemistry.22-66093
Abstract: Spectroscopic and microscopic techniques are complementary to electrochemical studies because electrochemical data consists of current, voltage and time, and has no direct information concerning the chemical structure of active species. Hence electrochemical in situ/operando spectroscopy and microscopy become powerful tools for identification of the electrochemically active species during the electrochemical reactions. The present comprehensive paper provides the fundamental theory, cell design concepts, and measurement tips of various spectroscopic and microscopic techniques. X-ray absorption spectroscopy, infrared spectroscopy, surface plasmon resonance, Raman spectroscopy, confocal microscopy and electron microscopy are covered in the present paper. The introduced cell design becomes the critical part for chemists and materials scientists to start these measurements. Several advanced techniques from recent studies are also introduced. (C) The Author(s) 2022. Published by ECSJ.
Type: article
URI: http://hdl.handle.net/2115/87527
Appears in Collections:理学院・理学研究院 (Graduate School of Science / Faculty of Science) > 雑誌発表論文等 (Peer-reviewed Journal Articles, etc)

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