Asymmetric hydrogenation of 1-phenylethenylboronic acid and esters for the synthesis of chiral organoboron compounds


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Title:	Asymmetric hydrogenation of 1-phenylethenylboronic acid and esters for the synthesis of chiral organoboron compounds
Authors:	Ueda, Masato Browse this author
	Saitoh, Atsushi Browse this author
	Miyaura, Norio Browse this author
Keywords:	Hydrogenation
	Asymmetric synthesis
	Boron and compounds
Issue Date:	18-Jan-2002
Publisher:	Elsevier Science B.V.
Journal Title:	Journal of Organometallic Chemistry
Volume:	642
Issue:	1-2
Start Page:	145
End Page:	147
Publisher DOI:	10.1016/S0022-328X(01)01239-6
Abstract:	The hydrogenation of ethanediol 1-phenylethenylboronic ester was carried out at −20 °C under a hydrogen atmosphere (9 atm) in the presence of [Rh(cod)2]BF4–(R)-BINAP (3 mol%). After alkaline hydrogen peroxide oxidation, the reaction gave 1-phenylethanol with 80% e.e.
Relation:	http://www.sciencedirect.com/science/journal/0022328X
Type:	article (author version)
URI:	http://hdl.handle.net/2115/15837
Appears in Collections:	工学院・工学研究院 (Graduate School of Engineering / Faculty of Engineering) > 雑誌発表論文等 (Peer-reviewed Journal Articles, etc)

Submitter: 宮浦憲夫

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