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Hokkaido University Collection of Scholarly and Academic Papers >
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Peer-reviewed Journal Articles, etc >
Synthesis of Sulfide Solid Electrolytes from Li2S and P2S5 in Anisole
| Title: | Synthesis of Sulfide Solid Electrolytes from Li2S and P2S5 in Anisole |
| Authors: | Maniwa, Riku Browse this author | | Calpa, Marcela Browse this author | | Rosero Navarro, Nataly Carolina Browse this author | | Miura, Akira Browse this author →KAKEN DB | | Tadanaga, Kiyoharu Browse this author →KAKEN DB |
| Issue Date: | 7-Jan-2021 |
| Publisher: | Royal Society of Chemistry |
| Journal Title: | Journal of Materials Chemistry A |
| Volume: | 9 |
| Issue: | 1 |
| Start Page: | 400 |
| End Page: | 405 |
| Publisher DOI: | 10.1039/D0TA08658D |
| Abstract: | We report the liquid-phase synthesis of sulfide solid electrolytes from Li2S and P2S5 using anisole at 200–300 °C under microwave radiation, in which -Li3PS4 and Li7P3S11 were directly precipitated in anisole in 30 min. Anisole afforded reasonable reactivity toward Li2S and P2S5 to form -Li3PS4 and Li7P3S11 powders at 200–300 °C. Moreover, a Li6PS5Cl precursor solution was synthesized from a Li3PS4–anisole suspension by adding ethanol, Li2S, and LiCl. The proposed synthesis using anisole is advantageous as a simple, short-time process and would be applicable for the production of all-solid-state batteries. |
| Type: | article (author version) |
| URI: | http://hdl.handle.net/2115/83765 |
| Appears in Collections: | 工学院・工学研究院 (Graduate School of Engineering / Faculty of Engineering) > 雑誌発表論文等 (Peer-reviewed Journal Articles, etc)
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Submitter: 三浦 章
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